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EFFECT OF PREPARATION METHOD ON PHYSICOCHEMICAL PROPERTIES OF NANOSTRUCTURED MgO POWDER

https://doi.org/10.29235/1561-8331-2018-54-3-281-288

Abstract

Magnesium oxide is widely used as an adsorbent, catalyst, identifier of chemical and toxic pollutants, in water and gas purification processes. Mesoporous magnesium oxide powder has been synthesized by the method of deposition, spray pyrolysis and glycine-citrate-nitrate method, their crystal structure, microstructure, granulometric composition and adsorption properties have been studied. Optimal conditions for the production of magnesium oxide by the glycine-citrate-nitrate method have been determined, which make it possible to obtain a powder with average primary particle sizes of 12 nm and the smallest sizes of secondary particles starting from 70 nm. The influence of the method of obtaining nanostructured magnesium oxide powder on the physicochemical properties is established. High values of the total pore volume of 1.038 cm3 /g exhibited the MgO powder obtained by the precipitation method.

About the Authors

I. V. Matsukevich
Institute of General and Inorganic Chemistry of the National Academy of Sciences of Belarus
Belarus

Irina V. Matsukevich – Ph. D. (Chemistry), Head of the Laboratory of the Magnesium Compounds

9/1, Surganov Str., 220072, Minsk



N. P. Krutko
Institute of General and Inorganic Chemistry of the National Academy of Sciences of Belarus
Belarus

Nikolay P. Krutko – Academician, D. Sc. (Chemistry), Head of the Department of Composite Material

9/1, Surganov Str., 220072, Minsk



L. V. Ovseenko
Institute of General and Inorganic Chemistry of the National Academy of Sciences of Belarus
Belarus

Ludmila V. Ovseenko – Ph. D. (Chemistry), Deputy Director for Science and Innovation

9/1, Surganov Str., 220072, Minsk



O. V. Polhovskaja
Institute of General and Inorganic Chemistry of the National Academy of Sciences of Belarus
Belarus

Olga V. Polhovskya – Laboratory Assistant, Laboratory of the Magnesium Compounds

9/1, Surganov Str., 220072, Minsk



D. V. Hubitski
Institute of General and Inorganic Chemistry of the National Academy of Sciences of Belarus
Belarus

Dzmitry V. Hubitski – Junior researcher, Laboratory of the Magnesium Compounds

9/1, Surganov Str., 220072, Minsk



V. V. Vashook
Institute of General and Inorganic Chemistry of the National Academy of Sciences of Belarus
Belarus

Vladimir V. Vashook – D. Sc. (Chemistry), Associate Professor, Leading Researcher

9/1, Surganov Str., 220072, Minsk



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ISSN 1561-8331 (Print)
ISSN 2524-2342 (Online)